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MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones

Santosh Shriram Katkar1, Amol Haridas Kategaonkar2, Kaluram N. Vidhate3
Affiliation: 
1 Department of Chemistry, MSS’s Arts, Science and Commerce College, Ambad, Dist Jalna-431 204 Maharashtra, India 2 Department of Chemistry, K.S.K.W. Arts, Science and Commerce College, CIDCO, Uttamnagar, Nashik-422 008, Maharashtra, India 3Department of Chemistry, Milind college of science, Nagsenwan Aurangabad, Maharashtra, India katkars25@gmail.com
DOI: 
https://doi.org/10.23939/chcht14.02.169
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Keywords:

Abstract: 
We have studied a series of mixed metal oxides of Mg-Al by a simple co-precipitation technique. Various characterization techniques, including XRD, SEM, EDS, TEM, BET and CO2-TPD were carried out to investigate their physicochemical properties. An efficient and facile protocol has been documented for the synthesis of chalcones using different aldehydes and acetophenone using Mg-Al oxide under reflux conditions in ethanol affording good to excellent yields. Recyclability of a catalyst is a significant feature of this protocol. Moreover, it was proposed that MgO can disperse and increase the basicity, pore size and catalytic activity.
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