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Визначення SF6 з використанням газової хроматографії з детектором захоплення електронів: порівняння сумішей СО2-N2 і CH4-Ar як допоміжного газу

Oman Zuas1, Harry Budiman1, Nuryatini Hamim2
Affiliation: 
1 Gas Analysis Laboratory (GasAL), Metrology in Chemistry Research Group, Research Centre for Chemistry-Indonesian Institute of Sciences (RCChem-LIPI), Kawasan PUSPIPTEK Serpong, 15314, Tangerang Selatan, Banten, Indonesia 2 Electrochemistry Laboratory (ELab), Metrology in Chemistry Research Group, Research Centre for Chemistry-Indonesian Institute of Sciences (RCChem-LIPI), Kawasan PUSPIPTEK Serpong, 15314, Tangerang Selatan, Banten, Indonesia oman.zuas@lipi.go.id
DOI: 
https://doi.org/10.23939/chcht11.04.420
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Keywords:

Abstract: 
Для визначення гексафлюору сульфуру (SF6) досліджено суміші 10% СО2-N2 і 5 % СН4-Ar як допоміжного газу в газовій хроматографії з детектором захоплення електронів (ГХ-ДЕЗ). Встановлено, що 10% СО2-N2 можна порівняти з 5 % CH4-Ar і така суміш може бути використана як альтернатива.
References: 

[1] Blasing T.: Recent Greenhouse Gas Concentrations. Oak Ridge National Laboratory. United State Department of Energy. http://cdiac.ornl.gov/pns/current_ghg.html
[2] Fang X., Hu X., Janssens-Maenhout G. et al.: Environ. Sci. Technol., 2013, 47, 3848. https://doi.org/10.1021/es304348x
[3] Santella N., Ho D., Schlosser P. et al.: Atmos. Environ., 2012, 47, 533. https://doi.org/10.1016/j.atmosenv.2011.09.012
[4] Jong E., Macekm P., Perera I. et al.: J. Chromatog. Sci., 2015, 53, 854. https://doi.org/10.1093/chromsci/bmu154
[5] Takase A., Kanoh H., Ohba T.: Sci. Rep., 2015, 5, 11994. https://doi.org/10.1038/srep11994
[6] Gandara M.: Mater. Technol., 2011, 45, 633.
[7] Asai K., Tsujimura M., Fantong W. et al.: Hydrol. Res. Lett., 2011, 5, 42. https://doi.org/10.3178/hrl.5.42
[8] Fang X., Thompson R., Saito T. et al.: Atmos. Chem. Phys., 2014, 14, 4779. https://doi.org/10.5194/acp-14-4779-2014
[9] Hall B., Dutton G., Mondeel D. et al.: Atmos. Meas. Tech., 2011, 4, 2441. https://doi.org/10.5194/amt-4-2441-2011
[10] http://kcdb.bipm.org/appendixb/ appbresults/ccqm-k15/ccqm-k15_final_report.pdf
[11] Peng X., Wang X., Huang Y.: Spectrosc. Spect. Anal., 2012, 32, 1535.
[12] Wells D., Hess P.: Method for Determination and Evaluation of Chlorinated Biphenyl (BPs) in Environmental Matrices. [in:] Barcelo D. (Ed.), Sample Handling and Trace Analysis of Pollutants: Techniques, Applications and Quality Assurance, 1st edn. Elsevier, Amsterdam 2000.
[13] Ussiri D., Lal R., Jarecki M.: Soil Till. Res., 2009, 104, 247. https://doi.org/10.1016/j.still.2009.03.001
[14] Wang Yi., Wang Yu., Ling H.: Adv. Atmos. Sci., 2010, 27, 1322. https://doi.org/10.1007/s00376-010-9212-2
[15] Zhang Y., Mu Y., Fang S. et al.: J. Environ. Sci. China, 2013, 25, 547. https://doi.org/10.1016/S1001-0742(12)60090-4
[16] ISO Guide 6142: Gas analysis – preparation of calibration gas mixtures – gravimetric method, 2001.
[17] Basavaiah K., Anil kumar U., Tharpa K. et al.: Iran. J. Chem. Chem. Eng., 2009, 28, 31.
[18] Budiman H., Zuas O.: Periodico Tche Quimica, 2015, 12, 7.
[19] Taverniers I., Loose M., Bockstaele E.: TrAC-Trend Anal. Chem., 2004, 23, 535.
[20] Linsinger T., Josephs R.: TrAC-Trend Anal. Chem., 2006, 25, 1125.
[21] Masson P.: J. Chrom. A, 2007, 158, 168. https://doi.org/10.1016/j.chroma.2007.03.003
[22] Walker R., Lumley I.: TrAC-Trend Anal. Chem., 1999, 18, 594.
[23] ISO Guide 33: Uses of certified reference materials, 2000.
[24] Nahid N.: Iran. J. Chem. Chem. Eng., 2002, 21, 80.
[25] Mcnair H., Miller J.: Basic Gas Chromatography. John Wiley & Sons, Inc, New York 1998.
[26] Shoeibi S., Iman M., Hossein R. et al.: Iran. J. Chem. Chem. Eng., 2013, 33, 21.
[27] Patnaik P.: Analysis of Organic Pollutants by Gas Chromatography. Lewis Publishers, Washington D.C. 1997.
[28] Kupiec T.: Int. J. Pharm. Comp., 2004, 8, 305.
[29] Barwick V.: J. Chrom. A, 1999, 849, 13. https://doi.org/10.1016/S0021-9673(99)00537-3
[30] Zuas O., Budiman H.: Hem. Ind., 2016, 70, 451. https://doi.org/10.2298/HEMIND150315051Z
[31] Zuas O., Budiman H.: Teknol. Indonesia, 2016, 39, 59.
[32] Kushwah D., Patel H.., Sinha P. et al.: E-J. Chem., 2011, 8, 1504. https://doi.org/10.1155/2011/462364
[33] AOAC. Guide 3: How to meet ISO 17025 requirements for method verification in the analytical laboratory accreditation criteria committee. Association of Official Analytical Chemists. http://www.aoac.org
[34] NATA. Guidelines for the validation and verification of quantitative and qualitative test methods. National Association of Testing Authorities. http://www.nata.com.au
[35] ICH-Guidelines-Q2A, Validation of analytical methods: definition and terminology. (CPMP/ICH/381/95). International Council for Harmonization. http://www.pharma.gally
[36] Budiman H., Hamim N., Zuas O.: Procedia Chem., 2015, 16, 465. https://doi.org/10.1016/j.proche.2015.12.080
[37] Hovind H., Magnusson B., Krysell M. et al.: Internal Quality Control–Handbook for chemical laboratories, NORDTEST Report TR 569, Nordic Innovation Stensberggata, Oslo, 4th edn., Norway 2011.
[38] Sousa S., Bialkowski S.: Anal. Chim. Acta, 2013, 433, 181. https://doi.org/10.1016/S0003-2670(01)00789-9
[39] Kim H., Yea S., Ro C. et al.: Bull. Korean Chem. Soc., 2002, 23, 301. https://doi.org/10.5012/bkcs.2002.23.2.301